Measurement of Solder Samples
SEA1200VX achieves highly sensitive results by measuring Pb-free solder samples at providing superior "limit of detection" and excellent repeatability.
Lead (Pb) in Pb Free Solder by SEA1200VX
Excellent linearity of the calibration curve for Pb-free solder created by optimal measurement conditions achieves a detection lower limit of 7.9ppm Pb at a measuring time of 300 seconds.
Excellent Repeatability
SEA1200VX achieves a significantly higher repeatability of CV 1.9 % at a measuring time of 100 seconds using an MBH Pb-free solder standard sample.
Measurement Conditions
Voltage: 40kV
Current: 1000µA
Collimator: φ8mm
Filter: for Pb
Meas Time: 100 sec.
Standard Sample
MBH 74X HA
Ave. (ppm) | 590 |
---|---|
Readings | 20 |
STDEV (ppm) | 11.3 |
CV% | 1.9 |
Concc. (ppm) | 615 |
Application to Real Samples
The following tables and graph show an example of a Pb-free solder measurement by SEA1200VX achieving better correlation with ICP-OES.
Measurement Conditions
Voltage: 40kV
Current: 1000µA
Collimator: φ8mm
Filter: for Pb
Time: 300 sec.
Comparison with ICP-OES and XRF data
Sample | ICP-OES | XRF |
---|---|---|
1 | 310 | 310 |
2 | 308 | 299 |
3 | 42.1 | 45.0 |
4 | 113 | 120 |
(unit: ppm)